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In this work two Co53.5Fe10X5.5B31 (X = Ta, W) alloys were synthesized from high purity (>= 99.9%) powder elements by means of mechanical alloying. In case of Ta-addition, mechanical alloying resulted in formation of two component material with nanocrystalline phase embedded in amorphous matrix. On the other hand, substitution of Ta by W retards partial amorphization induced by mechanical alloying. High pressure-temperature stability of both alloys was monitored using in situ energy dispersive X-rays.

In Situ Energy Dispersive X-Ray Diffraction Analysis of the Temperature-Pressure Stability of Co-Fe-(Ta, W)-B Alloys