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Diacerein and aceclofenac drug product combination is used for the pain management in osteoarthritis. The main aspects of the present study is to develop stability indicating, sensitive reverse phase high-performance liquid chromatographic method for the simultaneous determination of diacerein and ceclofenac in tablet dosage form. Were, the chromatographic separation was achieved on Kromasil C-18, 150 × 4.6 mm, 3.5-μm analytical column using mobile phase double distilled water (pH 2.7 with glacial acetic acid)-acetonitrile (45:55 v/v). Detector was set at 256 nm.

Sensitive LC method for the simultaneous determination of diacerein and aceclofenac in tablet dosage form