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In situ preparation of copper nanoparticles from a copper acetate precursor and its application as an efficient catalyst for the selective reduction of aromatic nitro compounds with hydrazine hydrate under combined microwave and ultrasound irradiation were described in detail. The results reveal the synergetic effect of microwave and ultrasound on the synthesis of copper nanoparticles, and formation of various amino derivatives.

Nano Cu-catalyzed efficient and selective reduction of nitroarenes under combined microwave and ultrasound irradiation