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Melt-compounded nanocomposites of synthetic styrene- co-butadiene rubber (BUNA SL18) and clay particles pretreated with three different modifiers were characterised by stretching calorimetry in the range of relative elongations λ &lt; 1.3. In contrast to the pristine rubber, all nanocomposites exhibited irreversibility of both mechanical work and heat effects in stretching/contraction cycles at fairly low elongations. The observed irreversibility was considered as evidence for chain slippage effects.

Thermoelastic Behaviour of Synthetic Rubber/Organoclay Nanocomposites at Low Elongations