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Single crystals of Tl 3 Sb 5 O 14  were grown by solid-state reaction in a corundum crucible under air (1273 K, 12 h). The structure was determined by single-crystal X-ray diffraction. It is isotypic to the K 3 Sb 5 O 14 , Rb 3 Sb 5 O 14  and Cs 3 Sb 5 O 14  analogues with orthorhombic  Pbam  symmetry and cell parameters  a  = 24.2899 (9) Å,  b  = 7.1931 (3) Å,  c  = 7.4182 (3) Å. The Sb atoms form irregular [SbO 6 ] octahedra, which are linked  via  edges and corners into a triperiodic network. The Tl +  ions are located in distinct channels of the network extending along [010] and [001].

The channel structure of trithallium pentaantimonate(V), Tl3Sb5O14

The channel structure of trithallium pentaantimonate(V), Tl₃Sb₅O₁₄