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The title coordination polymer, {[Co 2 (C 12 H 7 NO 8 )(H 2 O) 6 ]·5H 2 O}  n  , was crystallized at room temperature from an aqueous solution of 2-aminodi-acetic terephthalic acid (H 4 adtp) and cobalt(II) nitrate. The asymmetric unit consists of one adtp 4- ligand, one and two half Co II ions, six water ligands coordinated to Co II ions and five uncoordinated water mol-ecules. Two of the cobalt cations lie on centres of inversion and are coordinated in octa-hedral O 2 (OH 2 ) 4 environments, whereas the other adopts a slightly distorted octa-hedral NO 3 (OH 2 ) 2 environment. The crystal structure contains parallel stacked, one-dimensional zigzag chains, {[Co 2 (C 12 H 7 NO 8 )(H 2 O) 6 ]}  n  , which assemble into a three-dimensional supra-molecular architecture via networks of hydrogen bonds involving the coordinated and free water mol-ecules. One-dimensional 'water tapes' are formed, containing alternating six-membered and twelve-membered rings of water mol-ecules, together with water penta-mers, in which a central uncoordinated water mol-ecule is hydrogen bonded to two coordinated and two free water mol-ecules in a tetra-hedral arrangement.

acta crystallographica. section e, crystallographic communications

Synthesis and crystal structure of <i>catena</i>-poly[[hexaaqua{μ<sub>3</sub>-2-[bis(carboxylatomethyl)amino]terephthalato}dicobalt(II)] pentahydrate] containing water tapes and pentamers

Synthesis and crystal structure of catena-poly[[hexaaqua{μ3-2-[bis(carboxylatomethyl)amino]terephthalato}dicobalt(II)] pentahydrate] containing water tapes and pentamers

Synthesis and crystal structure of catena-poly[[hexaaqua{μ₃-2-[bis(carboxylatomethyl)amino]terephthalato}dicobalt(II)] pentahydrate] containing water tapes and pentamers