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Two new N -{[4-(3-aryl-4-sydnonyl-idene-amino)-5-sulfanyl-idene-1 H -1,2,4-triazol-3-yl]meth-yl}benzamides have been prepared by acid-promoted condensation reactions between 3-aryl-4-formyl-sydnones and N -[(4-amino-5-sulfanyl-idene-1 H -1,2,4-triazol-3-yl)meth-yl]benzamide, and both have been crystallized as ethanol monosolvates. N -{[4-(3-Phenyl-4-sydnonyl-idene-amino)-5-sulfanyl-idene-1 H -1,2,4-triazol-3-yl]meth-yl}benzamide ethanol monosolvate, C 19 H 15 N 7 O 3 S·C 2 H 6 O ( I ), and N -({4-[3-(4-methyl-phen-yl)-4-sydnonyl-idene-amino]-5-sulfanyl-idene-1 H -1,2,4-triazol-3-yl}meth-yl)benzamide ethanol monosolvate, C 20 H 17 N 7 O 3 S·C 2 H 6 O ( II ), differ only in the presence of a methyl group for ( II ) instead of a hydrogen atom for ( I ), and in both of them the ethanol component is disordered over two sets of atomic sites having occupancies of 0.836 (6) and 0.164 (6) in ( I ), and 0.906 (6) and 0.094 (6) in ( II ). Combinations of O-H⋯O and N-H⋯O hydrogen bonds link the mol-ecules into cyclic, centrosymmetric four-mol-ecule aggregates. Comparisons are made with the structures of some related compounds.

Two N-{[4-(3-aryl-4-sydnonylideneamino)-5-sulfanylidene-1H-1,2,4-triazol-3-yl]methyl}benzamides as disordered ethanol monosolvates