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The crystal structure of hydro-thermally synthesized ( T = 493 K, 7 d) caesium gallium bis-[hydrogen arsenate(V)], CsGa(HAsO 4 ) 2 , was solved by single-crystal X-ray diffraction. The compound crystallizes in the common RbAl(HAsO 4 ) 2 structure type ( R 32) and consists of a basic tetra-hedral-octa-hedral framework topology that houses Cs + cations in its channels. The AsO 4 tetra-hedron is disordered over two positions with site occupancy factors of 0.946 (1) and 0.054 (1). Strong hydrogen bonds strengthen the network. The structure was refined as inversion twin.

CsGa(HAsO4)2, the first Ga representative of the RbAl(HAsO4)2structure type

CsGa(HAsO₄)₂, the first Ga representative of the RbAl(HAsO₄)₂structure type