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Single crystals of Ti 8 Bi 9 O 0.25 , titanium bis-muth oxide (8/9/0.25), were obtained from a sample prepared by heating a mixture of Ti, TiO 2 and Bi powders in an Ar atmosphere. Single-crystal X-ray analysis revealed that the introduction of O atoms into the structure of Ti 8 Bi 9 retains the space-group type P 4/ nmm . The oxygen site is located within a Ti 4 tetra-hedron (point group symmetry m 2) that is vacant in the Ti 8 Bi 9 crystal structure. The occupancy of this site is 0.25 (4), and the O-Ti distance is 1.8824 (11) Å.

Crystal structure of Ti8Bi9O0.25 containing interstitial oxygen atoms

Crystal structure of Ti₈Bi₉O_0.25 containing interstitial oxygen atoms