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(II) has a distorted square-pyramidal coordination, involving two bridging O and two N atoms from a bisN,N’-(salicilidene)-1,3propanediaminato (SALPD) ligand as basal plane. One O atom from a dimethylformamide group for (I) and one O atom from a dioxane molecule for (II) complete the coordination number to five. The inner Cu ions have also irregular square-pyramidal environment, consisting of two bridging O atoms from a SALPD ligand, two bridging N atoms from two azido groups and one N atom from the third azido group. The Cu-N-Cu angles in the central azido bridges are 102.5(2) for (I) and 102.1(3)°. for (II). In (I) and (II), Cu-O-Cu angles in the O bridges have values 104.8(2) and 105.6(2)°.,respectively. The Cu-Cu distance in the azido bridge is 3.1462(7)Å for (I) and 3.1156(15)Å for (II). The Cu-Cu distances in the O bridges are 3.1501(7)Å and 3.1582(15)A in (I) and (II), respectively. Crystal data is given below: (I) [Cu(N3)2Cu(C17H16N2O2)(C3H7NO)],Triclinic P-1,9.211(1),10.394(2),12.941(1)Å, 77.831(1),92.293(2), 71.104(1)°., Iobs>2σ(I)= 3194, R=0.037; (II) [Cu(N3)2Cu(C17H16N2O2)(C4H8O2)], Monoclinic P21/n, 11.292(1),15.413(1),13.610(1)Å, β=97.402(5)°., Iobs>2σ(I)=2575,R= 0.07. Enraf-Nonius CAD-4, ω/2θ scans, MoKα 0.71073 Å

Crystal structure of platinum 2-methyl- and palladium 2,4-dimethyl-8-hydroselenoquinolinate