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011 of Mg or Al between the tetrahedral and octahedral sites is almost constant against Ga content in the MgAl2-xGaxO4 solid solution. A compositional variable of the Ga/(Mg+Ga) ratio in the octahedral site is not influenced by the occupancy of Al. The occupancy of Al is independent of the occupancy of Ga, though it depends on the occupancy of Mg according to thermal history. The local Al-O bond length in the tetrahedral site is 0.15 Å longer than the expected bond length. The nature that Al in spinel structure occupies mainly the octahedral site arises from the character of Al itself.

Soft synthesis and crystallographic characterization of calcium magnesium mixed carbonates