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24 European Crystallographic Meeting, ECM24, Marrakech, 2007 Page s189 Acta Cryst. (2007). A63, s189 (Grenoble) (λ=0.3748 Å) at 25 and 250C, respectively, suggests that the coefficient of thermal expansion is highest for samples with low iron substitution. Split of triangular Cu2 positions increases with temperature and the halfoccupied Cu2 positions from different coordination triangles approach one another, down to 2.70-2.75 Å in tennantite at 250C. There is insignificant residual electron density between the split Cu2 half-sites in tetrahedrite at 25C and its increase with temperature is moderate. The inter-site density is substantially higher in tennantite and it increases considerably with temperature, especially in the low-Fe sample.

Temperature dependent stability field of nanodomain structures in PZT ceramics using synchrotron powder diffraction