1,4,8,11‐Tetra­azacyclo­tetra­decane anti­mony(III) sulfide | Zendy

Lees Rachel J. E. | Zendy; Powell Anthony V. | Zendy; Watkin David J. | Zendy; Chippindale Ann M. | Zendy

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1,4,8,11‐Tetraazacyclotetradecane antimony(III) sulfide

Author(s) -

Lees Rachel J. E.,

Powell Anthony V.,

Watkin David J.,

Chippindale Ann M.

Publication year - 2007

Publication title -

acta crystallographica section c

Language(s) - English

Resource type - Journals

eISSN - 1600-5759

pISSN - 0108-2701

DOI - 10.1107/s010827010605044x

Subject(s) - amine gas treating , chemistry , antimony , molecule , sulfide , crystallography , stereochemistry , inorganic chemistry , computational chemistry , organic chemistry

Poly[1,4,8,11‐tetraazacyclotetradecane(2+) [hepta‐μ‐sulfido‐trisulfidohexaantimony(III)]], {(C 10 H 26 N 4 )[Sb 6 S 10 ]} n , consists of novel [Sb 6 S 10 ] 2− layers containing Sb 2 S 2 , Sb 4 S 4 and Sb 7 S 7 hetero‐rings, which are separated by macrocyclic amine molecules. The macrocyclic amine molecules are disordered over two crystallographically distinct positions and are diprotonated in order to balance the charge of the anionic layers.

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