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A highly efficient electrode material is required to explore and apply to microbial electrolysis cell (MEC) with high hydrogen evolution reaction (HER) efficiency. Pt/C was one of the most efficient catalysts for hydrogen production in current lab research, but it was expensive and some chemicals in wastewater were prone to Pt poisoning, which was a great limitation in application. Thus, a cheap and effective nickel(II) Oxide/Y (NiO/Y) material was prepared by using Y zeolites as carrier loaded with NiO in this study, which was used in MEC to evaluate the hydrogen evolution performance in comparison with Pt/C. The results indicated that NiO/Y composites showed a competitive HER performance to Pt/C. The linear sweep voltammetry (LSV) tests and Tafel plots showed that the NiO/Y composites exhibited the best catalytic activity for HER. In the MEC tests, the NiO/Y composites cathode was comparable with the Pt/C cathode in terms of current densities and energy efficiency. The coulombic efficiency, cathodic energy efficiency rate and hydrogen production rate obtained with NiO/Y cathode MEC was 85.88 ± 6.5%, 228.39 ± 3.2% and 0.83 ± 0.05 m 3 /m 3 d under, respectively, which were slightly higher than those obtained with the Pt/C cathode MEC. It was concluded that even with the cheap Y zeolites as the supports, the NiO/Y materials showed the superior performance, which was attributed to a good dispersing of the active component of NiO on the large specific surface area of Y zeolites and the fast escape of hydrogen bubbles from microporous and mesoporous structure of Y zeolites.

Cathodic hydrogen recovery using Y zeolites loaded nickel(II) Oxide instead of Pt/C in microbial electrolysis cell