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A Phosphine-free and effective process has been expressed for the formulation of  N , S -heterocycles following a C-N/C-S bond forming reactions. The described process operates through EDC-HCl-mediated heterocyclization of diverse isothiocyanates and bis-nucleophiles to deliver 1,3-thiazinone derivatives, which eliminates the use of hazardous reagents. The developed protocol was found applicable over a wide range of substrates in delivering  N , S -heterocycles in excellent yields at room temperature and short reaction time.

Synthesis of 4 H -3,1-Benzothiazin-4-Ones via C-N/C-S Bond Forming Reactions