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An efficient metal-free cyanoalkylation of 8-aminoquinoline and aniline-derived amides was achieved in the presence of K 2 S 2 O 8 . The method showed good substrate tolerance and also suitable for bromination and dimerization reactions.

Metal-free site-selective C–H cyanoalkylation of 8-aminoquinoline and aniline-derived amides with azobisisobutyronitrile