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HighlightsNiCo-LDHs successfully grow in situ on rod-like ZnO with unique structures.    The interface of NiCo@C and rod-like ZnO result in interfacial polarization.    The RLmin of NiCo@C/ZnO reaches − 60.97 dB with the EABmax of 6.08 GHz.    The excellent performance comes from the effect of dielectric loss and magnetic loss.Supplementary Information  The online version contains supplementary material available at 10.1007/s40820-021-00704-5.

Construction of 1D Heterostructure NiCo@C/ZnO Nanorod with Enhanced Microwave Absorption