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HighlightsA promising solar-powered environmentally friendly process for the synthesis and application of catalysts for hydrogen evolution reaction has been proposed.    A delicate NiCo(OH) x -Co y W catalyst with a bush-like heterostructure was realized via gas-template-assisted electrodeposition, followed by electrochemical etching process.    The excellent catalytic effect of NiCo(OH) x -Co y W for the hydrogen evolution reaction was systematically investigated through various physical and electrochemical analyses.Supplementary Information  The online version contains supplementary material available at 10.1007/s40820-021-00639-x.

Synergistic Interfacial and Doping Engineering of Heterostructured NiCo(OH)x-CoyW as an Efficient Alkaline Hydrogen Evolution Electrocatalyst