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HighlightsNitrogen was successfully incorporated in graphene nanowalls (CNWs) using cold gaseous plasma post-treatment and influence of nitrogen concentration and configuration in CNWs on electrical conductivity was demonstrated.    The mechanism of nitrogen incorporation was systematically studied using different characterisation techniques to make a bridge between established DFT theories.Electronic supplementary material  The online version of this article (10.1007/s40820-020-0395-5) contains supplementary material, which is available to authorized users.

N-Graphene Nanowalls via Plasma Nitrogen Incorporation and Substitution: The Experimental Evidence