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HighlightsAg 2 S NO delivery platforms maximize radiotherapy effects remarkably to inhibit the tumor growth.    Immunosuppressive tumor microenvironment was improved by Ag 2 S NO delivery system, significantly enhancing the anti-PD-L1 immune checkpoint blockade therapy.Electronic supplementary material  The online version of this article (10.1007/s40820-020-00431-3) contains supplementary material, which is available to authorized users.

Near-Infrared Light-Responsive Nitric Oxide Delivery Platform for Enhanced Radioimmunotherapy