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HighlightsA simple, but effective strategy is proposed to prepare Ti 3 C 2 T  x   MXene films by natural sedimentation method.    The enlarged interlayer spacing of the prepared films facilitates the accessibility of the lithium ions between the interlayers and thus leads to a greatly enhanced electrochemical performance.    The naturally sedimented MXene film shows a double lithium storage capacity compared to the conventional vacuum-filtered MXene film, along with improved rate performance and excellent cycle stability.Electronic supplementary material  The online version of this article (10.1007/s40820-020-00426-0) contains supplementary material, which is available to authorized users.

Enhanced Ionic Accessibility of Flexible MXene Electrodes Produced by Natural Sedimentation