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HighlightsSingle-atom Co–MoS 2  (SA Co–MoS 2 ) is prepared successfully to serve as a proof-of-concept nanozyme model, which exhibits peroxidase-like performance comparable to that of natural enzymes.    The different mechanisms between the single-atom metal center and the support are investigated experimentally and theoretically.Electronic supplementary material  The online version of this article (10.1007/s40820-019-0324-7) contains supplementary material, which is available to authorized users.

Revealing the Intrinsic Peroxidase-Like Catalytic Mechanism of Heterogeneous Single-Atom Co–MoS2