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HighlightsConstruct binder-free Ni@N-doped carbon nanospheres (Ni@N-CNSs) films were prepared and used as sulfur host.    N-doped carbon and nickel layer work together to suppress shuttle of polysulfides.    Ni@N-CNSs/S electrode shows enhanced rate performance and good cycling life.Electronic supplementary material  The online version of this article (10.1007/s40820-019-0295-8) contains supplementary material, which is available to authorized users.

Atomic Layer Deposition-Assisted Construction of Binder-Free Ni@N-Doped Carbon Nanospheres Films as Advanced Host for Sulfur Cathode