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A simple and scalable synthetic approach for one-step synthesis of graphene-CuO (TRGC) nanocomposite by an in situ thermo-annealing method has been developed. Using graphene oxide (GO) and copper hydroxide as a precursors reagent, the reduction of GO and the uniform deposition of in situ formed CuO nanoparticles on graphene was simultaneously achieved. The method employed no solvents, toxic-reducing agents, or organic modifiers. The resulting nanostructured hybrid exhibited improved H 2 S sorption capacity of 1.5 mmol H 2 S/g-sorbent (3 g S/100 g-sorbent). Due to its highly dispersed sub-20 nm CuO nanoparticles and large specific surface area, TRGC nanocomposite exhibits tremendous potential for energy and environment applications.

Facile In Situ Fabrication of Nanostructured Graphene–CuO Hybrid with Hydrogen Sulfide Removal Capacity