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In the study the mechanochemical synthesis was used to prepare photocatalytic materials based on TiO 2 , SiO 2,  and Fe 2 O 3 . During the preparation the impact of composition, milling speed, and calcination process on the properties of the composites was investigated. The structural and thermal properties of photocatalysts were determined using the N 2  adsorption/desorption, XRD, and FT-IR/PAS methods. The thermal stability of the obtained materials was also examined (TG/DTG). Moreover, their photocatalytic activity was tested in relation to Methylene Blue at UV and Vis radiation. The results indicate that the mechanochemical synthesis in the high-energy planetary mill is an effective method for obtaining materials with photocatalytic properties at the UV and Vis radiation. It was shown that the removal process of MB may be described by the pseudo-first-order kinetics.

Mechanochemical synthesis of nanophotocatalysts SiO2/TiO2/Fe2O3: their structural, thermal and photocatalytic properties