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The direct synthesis of H 2 O 2  from molecular H 2  and O 2  over AuPd catalysts, supported on TiO 2  and prepared via an excess chloride co-impregnation procedure is investigated. The role of Au:Pd ratio on the catalytic activity towards H 2 O 2  formation and its subsequent degradation is evaluated under conditions that have previously been found to be optimal for the formation of H 2 O 2 . The combination of relatively small nanoparticles, of mixed Pd-oxidation state is shown to correlate with enhanced catalytic performance. Subsequently, a detailed study of catalytic activity towards H 2 O 2  synthesis as a function of AuPd loading was conducted, with a direct correlation between catalytic activity and metal loading observed. Graphic Abstract

The Direct Synthesis of Hydrogen Peroxide over AuPd Nanoparticles: An Investigation into Metal Loading